Sounds like any of those days might have been useful, hmmm
Exactly - the acetic acid in the vinegar needs to dissolve the iron/steel completely fro best results and that takes a bit of time.
FWIW here's an original recipe for vinegar balk and how I've been doing it for the last 40 years:
Vinegar black aka vinegaroon aka ferric or ferrous nitrate
The original recipe:
VINEGAR BLACK
For giving color to the grain of leather there is no blacking that will at all compare with the well known vinegar black. This may be made in various ways. The simplest, and, without doubt, the best, is to procure shavings from an iron turner (note: some folks get the turnings from brake drums) and cover them with pure cider vinegar; heat up and set aside for a week or two, then heat again and set in a cool place for two weeks; pour off the vinegar, allow it to stand for a few days, and draw off and cork up in bottles. This will keep for a long time, and, while producing a deep black on leather, will not stain the hands.
How I do it most times:
I use de-oiled 4/0 steel wool: dip in acetone, squeeze out the extra and hang to dry - then tear or cut into small pieces. Add one pads worth of the de-oiled steel wool to one quart of white or cider vinegar - I use those plastic coffee "cans" and punch a single small hole in the lid to let off any gas buildup. Let it set in the hot sun which will speed the reaction. I let it set for about two weeks until there is only a light vinegar odor left and/or the bulk of the steel wool has been dissolved. About every couple of days I also stir the mix around so that it gets aerated - the mix needs oxygen to work best. I also keep a new batch "cooking" all the time so I have a constant supply.
For a deeper black, apply a bath of strong black tea first (this increase the tannins) and let it soak in good, then apply a generous amount of the vinegar black. Let set for about a half hour and then rinse with a mix of baking soda and warm water, about a 1/8 cup soda to a half gallon of water, dunk it in the mix or apply liberally with a sponge en let set for a few moments ONLY (too oong and you can "burn" the leather) and then rinse off with clean cool water. While still damp apply a light coat or two of your favorite saddle oil. Once dry top coat as normal
Experiment - I test a piece of each new side without oiling to see how well it takes the blacking, if need be I'll do a second black tea mix to darken, then apply the oil which also helps darken.
Instead of steel wool you can use chopped up bailing or fence wire - the smaller the better since it will dissolve in the vinegar bath faster.
BTW - this mix also makes a great "dye" for curly maple........